Electrodeposition of nickel and cobalt on AISI 304 stainless steel plates using the selective coating technique and ethaline as solvent

Authors

  • Nicole Baltodano-Obregon Facultad de Ingeniería Química, Universidad Nacional de Ingeniería (UNI), Managua, Nicaragua
  • Gregorio Vargas-Gutiérrez Centro de Investigación y de Estudios Avanzados (CINVESTAV), Unidad Saltillo Parque Industrial Santillo, México https://orcid.org/0000-0001-5315-7739

DOI:

https://doi.org/10.5377/nexo.v36i01.15796

Keywords:

Selective coating, AISI 304, Ethaline

Abstract

The electrochemical behaviour of cobalt and nickel chloride hexahydrate in ethaline was investigated by cyclic voltammetry at 30 °C. The results show that the reduction reaction of both elements is quasi reversible and occurs in a single two-electron transfer step. Electrodeposition by the selective coating technique of both elements on AISI 304 stainless steel was performed at -8.7 mA/cm2, 40 °C, and 40 min. The coating was characterised using scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray photoemitted electron spectrometry (XPS). The SEM and TEM images show the presence of a coating with a thickness of about 200 nm and the analysis by XPS confirms the presence of nickel and cobalt on the surface composition of the plate.

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Published

2023-02-22

How to Cite

Baltodano-Obregon, N., & Vargas-Gutiérrez, G. . (2023). Electrodeposition of nickel and cobalt on AISI 304 stainless steel plates using the selective coating technique and ethaline as solvent. Nexo Scientific Journal, 36(01), 38–52. https://doi.org/10.5377/nexo.v36i01.15796